Chemical synthesis in reaction autoclave

Reaction Autoclave

The reaction autoclave with a thermostat Julabo is used for a wide range of chemical syntheses from hydrogenation, hydrothermal syntheses to reactions at low temperatures. It is used especially in the cases when high temperature and pressure is needed.

Acquired information

• Carrying out of high-pressure and/or high temperature chemical synthesis
• Synthesis under optional atmosphere

Sample types

• Liquid or powder materials
• Inorganic, organic or coordination compounds

Modes, conditions and precision

• 3 reaction vessels can be used – stainless steel (50 mL) and two glass vessels (50 and 300 mL)
• Temperature range 0–220°C, depending on the vessel used
• The range of pressures from 1 up to 60 bars, depending on the vessel used
• Stirrer rotation up to 3000 min^–1
• Inert (e.g. N₂) or hydrogen atmosphere for hydrogenation reactions
• Possibility of sampling during a reaction
• Possibility of adding liquid or solid reactants during syntheses
• Changing and programming the temperature gradients in a given range (suitable for e.g. controlled crystallization)